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Improving the stability of beta-carotene and citral by nanoemulsions

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TitleInfo
Title
Improving the stability of beta-carotene and citral by nanoemulsions
Name (type = personal)
NamePart (type = family)
Yang
NamePart (type = given)
Xiaoqing
NamePart (type = date)
1981-
DisplayForm
Xiaoqing Yang
Role
RoleTerm (authority = RULIB)
author
Name (type = personal)
NamePart (type = family)
HUANG
NamePart (type = given)
QINGRONG
DisplayForm
QINGRONG HUANG
Affiliation
Advisory Committee
Role
RoleTerm (authority = RULIB)
chair
Name (type = personal)
NamePart (type = family)
HO
NamePart (type = given)
CHI-TANG
DisplayForm
CHI-TANG HO
Affiliation
Advisory Committee
Role
RoleTerm (authority = RULIB)
internal member
Name (type = personal)
NamePart (type = family)
Lee
NamePart (type = given)
Tung-Ching
DisplayForm
Tung-Ching Lee
Affiliation
Advisory Committee
Role
RoleTerm (authority = RULIB)
internal member
Name (type = personal)
NamePart (type = family)
Romsted
NamePart (type = given)
Larry
DisplayForm
Larry Romsted
Affiliation
Advisory Committee
Role
RoleTerm (authority = RULIB)
outside member
Name (type = corporate)
NamePart
Rutgers University
Role
RoleTerm (authority = RULIB)
degree grantor
Name (type = corporate)
NamePart
Graduate School - New Brunswick
Role
RoleTerm (authority = RULIB)
school
TypeOfResource
Text
Genre (authority = marcgt)
theses
OriginInfo
DateCreated (qualifier = exact)
2012
DateOther (qualifier = exact); (type = degree)
2012-10
CopyrightDate (qualifier = exact)
2012
Place
PlaceTerm (type = code)
xx
Language
LanguageTerm (authority = ISO639-2b); (type = code)
eng
Abstract (type = abstract)
In this study, various nanoemulsion formulations were prepared to encapsulate non-polar beta-carotene and partly polar flavor molecule citral. For the encapsulation of beta-carotene, the nanoemulsion core material was a mixture of both solid lipid (palm kernel fat) and liquid oil (medium chain triglyceride, MCT). Aqueous nanoemulsion dispersions were obtained by the combination of high speed and high pressure homogenization processes and the solid nanoemulsion powders were also obtained by lyophilization using sucrose as the cryoprotectant. For the aqueous dispersions, the formulation using pure palm kernel fat as the lipid phase was the best one to protect beta-carotene from degradation. For the freeze-dried samples, the incorporation of liquid MCT oil is necessary to disturb solid lipid crystallization to protect beta-carotene. The in vitro digestion experiments were performed to evaluate the bioaccessibility of beta-carotene in palm kernel fat nanoemulsion and MCT nanoemulsion; the results showed that the bioaccessibility of beta-carotene was greatly improved after encapsulation. The palm kernel fat had better performance than the MCT to release beta-carotene from the nanoemulsion formulations. For the encapsulation of citral, two strategies were developed to improve citral stability at acidic condition (pH = 3.0). The first strategy was to incorporate six different natural antioxidants (black tea extract, ascorbic acid, naringenin, tangeretin, beta-carotene and tanshinone) with citral together in the palm kernel fat nanoemulsions. The second strategy was to construct multilayer nanoemulsions to encapsulate citral. The multilayer emulsions were prepared by the layer-by-layer deposition technique between oppositely charged emulsion droplets and two polymer coatings: chitosan (CS) and ε-polylysine (EPL). The stability of citral as well as the production of the off-flavor compounds was analyzed by solid phase microextraction gas chromatography (SPME-GC). The results suggested that encapsulation of citral in combine with the appropriate antioxidants (beta-carotene, tanshinone and black tea extract) could greatly enhance citral’s chemical stability during storage; and the additional cationic chitosan interfacial layer was also effective to improve the stability of citral.
Subject (authority = RUETD)
Topic
Food Science
RelatedItem (type = host)
TitleInfo
Title
Rutgers University Electronic Theses and Dissertations
Identifier (type = RULIB)
ETD
Identifier
ETD_4231
PhysicalDescription
Form (authority = gmd)
electronic resource
InternetMediaType
application/pdf
InternetMediaType
text/xml
Extent
xi, 136 p. : ill.
Note (type = degree)
Ph.D.
Note (type = bibliography)
Includes bibliographical references
Note (type = vita)
Includes vita
Note (type = statement of responsibility)
by Xiaoqing Yang
Subject (authority = ETD-LCSH)
Topic
Beta carotene--Stability
Subject (authority = ETD-LCSH)
Topic
Emulsions
Identifier (type = hdl)
http://hdl.rutgers.edu/1782.1/rucore10001600001.ETD.000067032
RelatedItem (type = host)
TitleInfo
Title
Graduate School - New Brunswick Electronic Theses and Dissertations
Identifier (type = local)
rucore19991600001
Location
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NjNbRU
Identifier (type = doi)
doi:10.7282/T3B27T1X
Genre (authority = ExL-Esploro)
ETD doctoral
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Rights

RightsDeclaration (ID = rulibRdec0006)
The author owns the copyright to this work.
RightsHolder (type = personal)
Name
FamilyName
Yang
GivenName
Xiaoqing
Role
Copyright Holder
RightsEvent
Type
Permission or license
DateTime (encoding = w3cdtf); (qualifier = exact); (point = start)
2012-09-12 09:41:20
AssociatedEntity
Name
Xiaoqing Yang
Role
Copyright holder
Affiliation
Rutgers University. Graduate School - New Brunswick
AssociatedObject
Type
License
Name
Author Agreement License
Detail
I hereby grant to the Rutgers University Libraries and to my school the non-exclusive right to archive, reproduce and distribute my thesis or dissertation, in whole or in part, and/or my abstract, in whole or in part, in and from an electronic format, subject to the release date subsequently stipulated in this submittal form and approved by my school. I represent and stipulate that the thesis or dissertation and its abstract are my original work, that they do not infringe or violate any rights of others, and that I make these grants as the sole owner of the rights to my thesis or dissertation and its abstract. I represent that I have obtained written permissions, when necessary, from the owner(s) of each third party copyrighted matter to be included in my thesis or dissertation and will supply copies of such upon request by my school. I acknowledge that RU ETD and my school will not distribute my thesis or dissertation or its abstract if, in their reasonable judgment, they believe all such rights have not been secured. I acknowledge that I retain ownership rights to the copyright of my work. I also retain the right to use all or part of this thesis or dissertation in future works, such as articles or books.
RightsEvent
DateTime (encoding = w3cdtf); (qualifier = exact); (point = start)
2012-10-31
DateTime (encoding = w3cdtf); (qualifier = exact); (point = end)
2013-10-31
Type
Embargo
Detail
Access to this PDF has been restricted at the author's request. It will be publicly available after October 31st, 2013.
Copyright
Status
Copyright protected
Availability
Status
Open
Reason
Permission or license
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