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Morphological control of multifunctional melting gel coatings via electrospray deposition

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TitleInfo
Title
Morphological control of multifunctional melting gel coatings via electrospray deposition
Name (type = personal)
NamePart (type = family)
Gamboa
NamePart (type = given)
Arielle Marie
DisplayForm
Gamboa, Arielle Marie
Role
RoleTerm (authority = RULIB); (type = text)
author
Name (type = personal)
NamePart (type = family)
Singer
NamePart (type = given)
Jonathan P
DisplayForm
Jonathan P Singer
Affiliation
Advisory Committee
Role
RoleTerm (authority = RULIB)
chair
Name (type = corporate)
NamePart
Rutgers University
Role
RoleTerm (authority = RULIB)
degree grantor
Name (type = corporate)
NamePart
School of Graduate Studies
Role
RoleTerm (authority = RULIB)
school
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Text
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theses
OriginInfo
DateCreated (encoding = w3cdtf); (keyDate = yes); (qualifier = exact)
2020
DateOther (encoding = w3cdtf); (qualifier = exact); (type = degree)
2020-05
Language
LanguageTerm (authority = ISO 639-3:2007); (type = text)
English
Abstract (type = abstract)
Melting gels are a class of hybrid organic-inorganic gels prepared via the sol-gel process that have glass transition temperatures near room temperature and consolidation temperatures ~150┬░C. Their thermal properties allow for useful processing techniques: melting gels exhibit thermoplastic behavior below their consolidation temperatures, then undergo complete cross-linking to form organically modified silica networks upon consolidation. By appropriately tuning surface properties, these glass sprays can be used as protective coatings in electronics and anti-corrosion in metals. Electrospray deposition was used to spray dilute solutions of 1 wt% melting gels in 2-butanone onto silicon substrates. Electrospray uses high voltages to produce charged, monodisperse droplets, and because of the low solid contents used in our study, it uniformly delivers small amounts of melting gel at a continuous rate. Parameters such as the pH of melting gel synthesis, solution viscosity, and spray polarity can be varied to alter and study the effects of charge injection on the consolidation of the melting gel into hybrid glasses. Optical images, film thickness measurements, nanoindentation, FT-IR, and goniometry were used to evaluate and demonstrate the effects of these variables on both the physical morphology along with the chemical structure of the final coatings.
Subject (authority = RUETD)
Topic
Mechanical and Aerospace Engineering
RelatedItem (type = host)
TitleInfo
Title
Rutgers University Electronic Theses and Dissertations
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ETD
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ETD_10890
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application/pdf
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text/xml
Extent
1 online resource (vii, 52 pages)
Note (type = degree)
M.S.
Note (type = bibliography)
Includes bibliographical references
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Title
School of Graduate Studies Electronic Theses and Dissertations
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rucore10001600001
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NjNbRU
Identifier (type = doi)
doi:10.7282/t3-yt1j-r755
Genre (authority = ExL-Esploro)
ETD graduate
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RightsDeclaration (ID = rulibRdec0006)
The author owns the copyright to this work.
RightsHolder (type = personal)
Name
FamilyName
Gamboa
GivenName
Arielle Marie
Role
Copyright Holder
RightsEvent
Type
Permission or license
DateTime (encoding = w3cdtf); (qualifier = exact); (point = start)
2020-04-29 17:20:32
AssociatedEntity
Name
Arielle Marie Gamboa
Role
Copyright holder
Affiliation
Rutgers University. School of Graduate Studies
AssociatedObject
Type
License
Name
Author Agreement License
Detail
I hereby grant to the Rutgers University Libraries and to my school the non-exclusive right to archive, reproduce and distribute my thesis or dissertation, in whole or in part, and/or my abstract, in whole or in part, in and from an electronic format, subject to the release date subsequently stipulated in this submittal form and approved by my school. I represent and stipulate that the thesis or dissertation and its abstract are my original work, that they do not infringe or violate any rights of others, and that I make these grants as the sole owner of the rights to my thesis or dissertation and its abstract. I represent that I have obtained written permissions, when necessary, from the owner(s) of each third party copyrighted matter to be included in my thesis or dissertation and will supply copies of such upon request by my school. I acknowledge that RU ETD and my school will not distribute my thesis or dissertation or its abstract if, in their reasonable judgment, they believe all such rights have not been secured. I acknowledge that I retain ownership rights to the copyright of my work. I also retain the right to use all or part of this thesis or dissertation in future works, such as articles or books.
Copyright
Status
Copyright protected
Availability
Status
Open
Reason
Permission or license
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Technical

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ETD
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windows xp
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1.7
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2020-05-04T14:32:16
DateCreated (point = end); (encoding = w3cdtf); (qualifier = exact)
2020-05-04T14:32:16
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